E.I.
|
Mẫu thịt, sản phẩm thịt
|
|
|
|
-
|
Các chỉ tiêu chất lượng sản phẩm
|
03-07
|
-
|
Ẩm (**) (a)
|
NMKL No.23.1991
|
Định lượng
|
|
-
|
Định tính Axit boric và muối borate (**) (a)
|
05.2/CL1/ST 03.45
(TCVN 8895:2012)
|
0,1%
|
|
-
|
Các chất chuyển hóa nhóm nitrofuran
|
|
|
03-07
|
-
|
Nitrofuran (AOZ) (**)(a)
|
05.2/CL1/ST 03.69
(LC-MS/MS)
Ref: Analysis of Nitrofuran Metabolites in Tilapia Using Agilent 6410 Triple Quadrupole
|
0,2 µg/kg
|
|
-
|
Nitrofuran (AMOZ) (**)(a)
|
0,2 µg/kg
|
|
-
|
Nitrofuran (SEM, AHD) (**)(a)
|
0,5 µg/kg
|
|
-
|
Nhóm phenicol
|
|
|
03-07
|
-
|
Chloramphenicol (CAP) (**) (a)
|
05.2/CL1/ST 03.68
(LC-MS/MS)
Ref: Agilent 5989-5975EN
|
0,1 µg/kg
|
|
-
|
Florfenicol (**)
|
0,3 µg/kg
|
|
-
|
Nhóm Tetracycline
|
|
|
03-07
|
-
|
Tetracycline (**)(a)
|
05.2/CL1/ST 03.82
(LC-MS/MS)
Ref: Determination of Multi-Residue Tetracyclines and their Metabolites in Milk by High Performance Liquid Chromatography - Tandem Mass Spectrometry, Agilent
|
20 µg/kg
|
|
-
|
Oxytetracyclin (**)(a)
|
20 µg/kg
|
|
-
|
Chlortetracyclin (**)(a)
|
20 µg/kg
|
|
-
|
Doxycyclin (**)(a)
|
1,0 µg/kg
|
|
-
|
Nhóm Aflatoxin
|
|
|
03-07
|
-
|
Aflatoxin G1
|
05.2-CL1/ST 3.44
(HPLC-FLD)
Ref: AOAC 994.08; AOAC 991.31; AOAC 971.22 (49-2-03)
|
0,30 µg/kg
|
|
-
|
Aflatoxin G2
|
0,30 µg/kg
|
|
-
|
Aflatoxin B1
|
0,15 µg/kg
|
|
-
|
Aflatoxin B2
|
0,15 µg/kg
|
|
-
|
Nhóm chất tạo nạc (beta-agonist)
|
|
|
03-07
|
-
|
Salbutamol (**) (a)
|
05.2/CL1/ST 03.75
(LC-MS/MS)
Ref: Determination of β2-Agonists in Pork Using Agilent SampliQ SCX Solid-Phase Extraction Cartridges and Liquid Chromatography-Tandem Mass Spectrometry.
|
Thịt, gan, thận: 0,2 µg/kg
|
|
-
|
Clenbuterol (**) (a)
|
|
-
|
Ractopamine (**) (a)
|
|
-
|
Kim loại
|
|
|
03-07
|
-
|
Arsen (As) (**)(a)
|
05.2/CL1/ST 03.67
(ICP/MS)
Ref: AOAC 999.10
|
0,010 mg/kg
|
|
-
|
Cadimi (Cd) (**)(a)
|
0,010 mg/kg
|
|
-
|
Chì (Pb) (**)(a)
|
0,010 mg/kg
|
|
-
|
Đồng (Cu) (**)(a)
|
0,400 mg/kg
|
|
-
|
Kẽm (Zn) (**)(a)
|
13,300 mg/kg
|
|
-
|
Thủy ngân (Hg) (**)(a)
|
0,005 mg/kg
|
|
-
|
Niken (Ni) (**)(a)
|
0,015 mg/kg
|
|
-
|
Nhóm Sulfonamide
|
|
|
03-07
|
-
|
Sulfadiazine (**)(a)
|
05.2/CL1/ST 03.70
(LC-MS/MS)
Ref: Determination of Sulfonamide antibiotic in Bovine liver using Agilent Bond elut QuEchers en kits by LC/MS/MS
|
10 µg/kg
|
|
-
|
Sulfamethazine (Sulfadimidin) (**)(a)
|
-
|
Sulfachloropyridazine (**)(a)
|
-
|
Sulfamethoxazole (**)(a)
|
-
|
Sulfadimethoxine (**)(a)
|
-
|
Nhóm Quinolones
|
|
|
03-07
|
-
|
Flumequine (**)(a)
|
05.2/CL1/ST 03.71
(LC-MS/MS)
Ref: Determination of Quinolone Antibiotics in Bovine liver using Agilent bond elut Quechers kit by LC-MS/MS
|
5,0 µg/kg
|
|
-
|
Ciprofloxacin (**)(a)
|
-
|
Enrofloxacin (**)(a)
|
-
|
Sarafloxacin (**)(a)
|
-
|
Auramine (**)(a)
|
05.2/CL1/ST 03.87
(LC-MS/MS)
Ref: Journal of Chromatography B, 879 (2011) 2416– 2422
|
3,0 µg/kg
|
|
E.II
|
Mẫu thực vật (rau, củ, quả, chè, cà phê,…)
|
|
|
-
|
Các chỉ tiêu chất lượng sản phẩm
|
|
-
|
Ẩm (**) (a)
|
NMKL No.23.1991
|
Định lượng
|
03-07
|
-
|
Định tính Axit boric và muối borate (**) (a)
|
05.2/CL1/ST 03.45
(TCVN 8895:2012)
|
0,1%
|
03-07
|
-
|
Nitrit (**)(a)
|
05.2/CL1/ST 03.47
(TCVN 7767:2007)
|
1 mg/kg
|
03-07
|
-
|
Nitrate (**)(a)
|
1 mg/kg
|
03-07
|
-
|
Nhóm Aflatoxin (mẫu ngũ cốc)
|
|
|
03-07
|
-
|
Aflatoxin G1 (a)(**)
|
05.2-CL1/ST 3.44
(HPLC-FLD)
Ref: AOAC 994.08; AOAC 991.31; AOAC 971.22 (49-2-03)
|
0,5 µg/kg
|
|
-
|
Aflatoxin G2 (a) (**)
|
0,5 µg/kg
|
|
-
|
Aflatoxin B1 (a) (**)
|
0,3 µg/kg
|
|
-
|
Aflatoxin B2 (a) (**)
|
0,3 µg/kg
|
|
-
|
TBVTV nhóm chlor hữu cơ
|
|
|
03-07
|
-
|
Gamma-Lindane (**)(a)
|
05.2/CL1/ST 03.54
(GC/MS)
Ref: AOAC 2007.01
|
0,01 mg/kg
|
|
-
|
Heptachlor (**)(a)
|
0,01 mg/kg
|
|
-
|
Hexachlorbenzen(**)(a)
|
0,01 mg/kg
|
|
-
|
Aldrin (**)(a)
|
0,01 mg/kg
|
|
-
|
Eldrin (**)(a)
|
0,01 mg/kg
|
|
-
|
Dieldrin (**)(a)
|
0,01 mg/kg
|
|
-
|
Trans-Chlordane (**)(a)
|
0,01 mg/kg
|
|
-
|
Cis-Chlordane (**)(a)
|
0,01 mg/kg
|
|
-
|
4,4’-DDT (**)(a)
|
0,04 mg/kg
|
|
-
|
α, β -Endosulfan(**)(a)
|
05.2/CL1/ST 03.58
(GC/MS)
Ref: AOAC 2007.01
|
0,01 mg/kg
|
|
-
|
Chlorothanonil (**)(a)
|
0,01 mg/kg
|
|
-
|
Fipronil (**)(a)
|
0,01 mg/kg
|
|
-
|
Fipronil
|
05.2/CL1/ST 03.84
(LC/MSMS)
Ref: method of test for pesticide residues in foods- multiresidue analysis- Taiwan food and drug administration correction annoucement No. 1031900615. (2014- 0703)
|
0,0006 mg/kg
|
|
-
|
Dichloran (**)(a)
|
05.2/CL1/ST 03.66
(GC/MS)/
Ref: AOAC 2007.01
|
0,01 mg/kg
|
|
-
|
Thuốc trừ sâu gốc Phosphor (rau, củ, quả, chè)
|
|
|
03-07
|
-
|
Chlorpyrifos (**)(a)
|
05.2/CL1/ST 03.58
(GC/MS)
Ref: AOAC 2007.01
|
0,01 mg/kg
|
|
-
|
Quinalphos (**)(a)
|
0,01 mg/kg
|
|
-
|
Profenofos (**)(a)
|
0,01 mg/kg
|
|
-
|
Chlorpyrifos Methyl (**)(a)
|
05.2/CL1/ST 03.66
(GC/MS)
Ref: AOAC 2007.01
|
0,01 mg/kg
|
|
-
|
Malathion (**)(a)
|
0,01 mg/kg
|
|
-
|
Triazophos (**)(a)
|
0,01 mg/kg
|
|
-
|
Trichlorfon (**)(a)
|
05.2/CL1/ST 03.72
(LC-MS/MS)
|
0,01 mg/kg
|
|
-
|
Acephate (**)
|
05.2/CL1/ST 03.76
(LC-MS/MS)
Ref: AOAC 2007.01
|
0,005 mg/kg
|
|
-
|
Methamidophos (**)
|
0,005 mg/kg
|
|
-
|
Nhóm Carbamat (rau, củ, quả, chè)
|
|
|
03-07
|
-
|
Aldicarb (**)(a)
|
05.2/CL1/ST 03.72
(LC-MS/MS)
Ref: AOAC 2007.01
|
0,01 mg/kg
|
|
-
|
Carbendazime (**)(a)
|
0,01 mg/kg
|
|
-
|
Carbosulfan (**)(a)
|
05.2/CL1/ST 03.58
(GC/MS)
Ref: AOAC 2007.01
|
0,01 mg/kg
|
|
-
|
Indoxacarb (**)(a)
|
0,10 mg/kg
|
|
-
|
Nhóm Cúc (rau, củ, quả, chè)
|
|
|
03-07
|
-
|
Cis/trans-Permethrin (**)(a)
|
05.2/CL1/ST 03.58
(GC/MS)
Ref: AOAC 2007.01
|
0,01 mg/kg
|
|
-
|
α,β– Cypermethrin (**)(a)
|
0,02 mg/kg
|
|
-
|
Fenvalerate (**)(a)
|
0,01 mg/kg
|
|
-
|
Cyfluthrin (**)(a)
|
0,05 mg/kg
|
|
-
|
Bifenthrin (**)(a)
|
05.2/CL1/ST 03.66
(GC/MS)
Ref: AOAC 2007.01
|
0,01 mg/kg
|
|
-
|
Fenpropathrin (**)(a)
|
0,01 mg/kg
|
|
-
|
λ-Cyhalothrin (**)(a)
|
0,01 mg/kg
|
|
-
|
Deltamethrin (**)(a)
|
0,01 mg/kg
|
|
-
|
Nhóm Triazole (rau, củ, quả, chè)
|
|
|
03-07
|
-
|
Propiconazole (**)(a)
|
05.2/CL1/ST 03.58
(GC/MS)
Ref: AOAC 2007.01
|
0,01 mg/kg
|
|
-
|
Hexaconazole (**)(a)
|
0,01 mg/kg
|
|
-
|
Difenoconazole (**)(a)
|
0,10 mg/kg
|
|
-
|
Tetraconazole (**)(a)
|
05.2/CL1/ST 03.66
(GC/MS)
Ref: AOAC 2007.01
|
0,01 mg/kg
|
|
-
|
Cyproconazole (**)(a)
|
0,01 mg/kg
|
|
-
|
Thiabendazole (**)(a)
|
05.2/CL1/ST 03.72
(LC-MS/MS)
Ref: AOAC 2007.01
|
0,01 mg/kg
|
|
-
|
Fenbuconazoleb (**)(a)
|
0,01 mg/kg
|
|
-
|
Nhóm Imidazole (rau, củ, quả, chè)
|
|
|
03-07
|
-
|
Imidaclorpid (**)(a)
|
05.2/CL1/ST 03.72
(LC-MS/MS)
Ref: AOAC 2007.01
|
0,01 mg/kg
|
|
-
|
Imidaclorpid (**)
|
05.2/CL1/ST 03.76
(LC-MS/MS)
Ref: AOAC 2007.01
|
0,005 mg/kg
|
|
-
|
Nhóm Avermectin (rau, củ, quả, chè)
|
|
|
03-07
|
-
|
Abamectin (**)
|
05.2/CL1/ST 03.85
(LC-MS/MS)
Ref: AOAC 2007.01
|
0,01 mg/kg
|
|
-
|
Emamectin benzoate (**)
|
0,01 mg/kg
|
|
-
|
Nhóm khác (rau, củ, quả)
|
|
|
03-07
|
-
|
Metalaxyl (**)(a)
|
05.2/CL1/ST 03.58
(GC/MS)
Ref: AOAC 2007.01
|
0,01 mg/kg
|
|
-
|
Kresoxim- methyl (**)(a)
|
05.2/CL1/ST 03.72
(LC-MS/MS)
Ref: AOAC 2007.01
|
0,01 mg/kg
|
|
-
|
Kim loại (Nông sản khô-chè, cà phê,…)
|
|
|
03-07
|
-
|
Arsen (As) (**)(a)
|
05.2/CL1/ST 03.67
(ICP/MS)
Ref: AOAC 999.10
|
0,01 mg/kg
|
|
-
|
Cadimi (Cd) (**)(a)
|
0,01 mg/kg
|
|
-
|
Chì (Pb) (**)(a)
|
0,01 mg/kg
|
|
-
|
Đồng (Cu) (**)(a)
|
0,20 mg/kg
|
|
-
|
Kẽm (Zn) (**)(a)
|
1,90 mg/k
|
|
-
|
Thủy ngân (Hg) (**)(a)
|
0,005 mg/kg
|
|
-
|
Niken (Ni) (**)(a)
|
0,20 mg/kg
|
|
-
|
Kim loại (Nông sản tươi-rau, quả)
|
|
|
03-07
|
-
|
Arsen (As) (**)(a)
|
05.2/CL1/ST 03.67
(ICP/MS)
Ref: AOAC 999.10
|
0,010 mg/kg
|
|
-
|
Cadimi (Cd) (**)(a)
|
0,010 mg/kg
|
|
-
|
Chì (Pb) (**)(a)
|
0,010 mg/kg
|
|
-
|
Đồng (Cu) (**)(a)
|
0,250 mg/kg
|
|
-
|
Kẽm (Zn) (**)(a)
|
1,100 mg/kg
|
|
-
|
Thủy ngân (Hg) (**)(a)
|
0,005 mg/kg
|
|
-
|
Niken (Ni) (**)(a)
|
0,020 mg/kg
|
|
-
|
Các chất khác
|
|
|
|
-
|
Caffein (**)
|
ISO 20481:2008 (HPLC-PDA)
|
LOQ: 0,01%
|
03-07
|
-
|
Lưu huỳnh (**)
|
05.2/CL1/ST 03.81
(UV-Vis)
|
LOQ: 0,1%
|
03-07
|
-
|
Patulin (nước ép quả) (**)(a)
|
TCVN 8161:2009
(HPLC-PDA)
|
-
µg/kg
(nước táo)
|
03-07
|
-
|
Auramine (**)(a)
|
05.2/CL1/ST 03.87
(LC-MS/MS)
Ref: Journal of Chromatography B, 879 (2011) 2416– 2422
|
3,0 µg/kg
|
03-07
|
-
|
Xác định hàm lượng đa dư lượng (43 chất) thuốc bảo vệ thực vật: (**)
Methamidophos; Carbaryl; Fenobucarb; Ethoprophos; Trifluralin; Hexachlorbenzen; Dichloran; Ethoxyquine; Lindane (gamma HCH); Chlorpyrifos methyl; Metalaxyl; Heptachlor; Malathion; Chlorpyrifos; Aldrin; Tetraconazole; Fipronil; Quinalphos; Methidathion; Cis-Chlordane; Trans-Chlordane; Endrin; alpha Endosulfan; Hexaconazole; Profenofos; Dieldrin; beta Endosulfan; 4-4’ DDT; Propiconazole II; Propiconazole I; Propargite; Bifenthrin; Fenproparthrin; lamda Cyhalothrin II; lamda Cyhalothrin I; Permethrin; Cypermethrin; Flucythrinate; Fenvalerate;
|
AOAC 2007.01
(GC-MSMS)
|
0,005mg/kg
|
03-07
|
Cyfluthrin
|
0,025 mg/kg
|
03-07
|